Technical Specification

Make

Bruker

Model

AVANCE III HD

Frequency

400 MHz

Magnetic Field

9.4 Tesla

Major Specifications / Accessories available

a) 5 mm BBO probe with gradient facility and auto sampler with VT facility. Tuning range from ¹⁰⁹Ag to ³¹P also observation of ¹⁹F with ¹H decoupling.

b) 4 mm CP/MAS probe with VT facility. Tuning range from ¹⁵N to ³¹P +¹H.

Type of measurements / Analysis available

1D NMR, 2D NMR, Multi-nuclear NMR; Variable temperature measurements.

Sample Requirement

Liquid Sample

5 mg for ¹H NMR and 50 mg for ¹³C NMR experiment. Compounds should be highly pure and soluble in commonly available solvents . Solubility, nature of compound [carcinogenic, toxic, lachrymatory, explosive, hygroscopic] and Structural formula [contemplated / known] to be mentioned. The sample must be soluble in 0.6 ml of deuterated solvent. Facilities available for 1D NMR, 2D NMR, Multi-nuclear NMR; Variable temperature measurements. RADIOACTIVE MATERIAL should not be submitted.

Solid Sample

For Solid State NMR, 750 mg fine powder is required.